ACID DIGESTION
Samples are dried at 105°C (50°C for determination of mercury). Acid digestion is performed with a mixture of nitric, hydrochloric and hydrofluoric acid in sealed teflon containers in a microwave system. Samples are centrifuged before analysis. Acid digestion is used because certain elements are lost when exposed to the fusion process.
MG-2 includes determination of As, Cd, Co, Cu, Hg, Ni, Pb, S and Zn after acid digestion while other elements are determined after fusion. In
M-5, all constituent elements are determined after acid digestion.